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| | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | BRITISH STANDARD BS EN 12099 1997 BS 2782 Part 11 1103E 1997 The European Standard EN 12099 1997 has the status of a British Standard ICS 23.040.20; 23.040.45; NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW Plastics piping systems Polyethylene piping materials and components Determination of volatile content This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 December 1997 BSI 1997 ISBN 0 580 28748 3 BS EN 12099 1997 Amendments issued since publication Amd. No.DateText affected National foreword This British Standard is the English language version of EN 12099 1997 published by the European Committee for Standardization CEN. The UK participation in its preparation was entrusted to Technical Committee PRI/61, Plastics piping systems and components, which has the responsibility to aid enquirers to understand the text; present to the responsible European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests ined; monitor related international and European developments and promulgate them in the UK. A list of organizations represented on this committee can be obtained on request to its secretary. This European Standard is also incorporated into BS 2782 s of testing plastics Part 11 Thermoplastics pipes, fitting and valves, as 1103E 1997, for association with related test s for plastics materials and plastics piping systems. It is also for use for the revision or amendment of other national standards as practicable, but it should not be presumed to apply to any existing standard or specification which contains or makes reference to a different test until that standard/specification has been amended or revised to make reference to this and any requirements adjusted as appropriate. NOTE Subclause 4.1 states that test pieces may be cut from a cross-section of a pipe or fitting. For a test for determining the content of volatile material, it is essential that the cutting technique does not heat the test piece to an extent that would expel any material and thereby affect the results. In the absence of any related instructions by a referring standard, the responsible BSI committee considers that the cutting should not induce any tangible heating or involve any coolant which could be adsorbed. Warning note. This British Standard, which is identical with EN 12099 1997, does not necessarily detail all the precautions necessary to meet the requirements of the Health and Safety at Work etc. Act 1974. Attention should be paid to any appropriate safety precautions and the should be operated only by trained personnel. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 4, an inside back cover and a back cover. CEN European Committee for Standardization Comite Europe en de Normalisation Europa isches Komitee fu r Normung Central Secretariat rue de Stassart 36, B-1050 Brussels 1997 CEN All rights of exploitation in any and by any means reserved worldwide for CEN national Members. Ref. No. EN 12099 1997 E EUROPEAN STANDARDEN 12099 NORME EUROPE ENNE EUROPA ISCHE NORM May 1997 ICS Descriptors Fluid pipelines, plastics tubes, polyethylene, chemical analysis, determination of content, volatile matter English version Plastics piping systems Polyethylene piping materials and components Determination of volatile content Syste mes de canalisations en plastiques Mate riaux et composants de tuyauterie en polye thyle ne De termination de la teneur en matie res volatiles Kunststoff-Rohrleitungssysteme Polyethylen-Rohrleitungswerkstoffe und teile Bestimmung des Gehalts an flu chtigen Bestandteilen This European Standard was approved by CEN on 1997-03-28. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standard exists in three official versions English, French, German. A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. Page 2 EN 12099 1997 BSI 1997 Foreword This European standard has been prepared by Technical Committee CEN/TC 155, Plastics piping systems and ducting systems, the secretariat of which is held by NNI. The material-dependent parameters and/or perance requirements are incorporated in the System Standards concerned. This standard is one of a series of standards on test s which support System Standards for plastics piping systems and ducting systems. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by November 1997, and conflicting national standards shall be withdrawn at the latest by November 1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. w w w . b z f x w . c o m Page 3 EN 12099 1997 BSI 1997 1 Scope This standard specifies a for determining the content of material volatile at 105 C in polyethylene PE piping materials. This is applicable to moulding and extrusion materials. It can also be applicable to components in PE piping systems. 2 Principle The consists of determining the loss of mass of a test piece which has been put in a drying oven at a given temperature. NOTE. It is assumed that the following test parameters are set by the standard making reference to this standard a the source and of the test piece see 4.1; b number of test pieces see 4.2. 3 Apparatus 3.1 Drying oven or equivalent device, capable of maintaining the temperature at 1052 C at the position for the cups see 3.2 and 5.4. 3.2 A cylindrical glass weighing cup, with a diameter of 35 mm capable of containing a test piece see 4.1, a minimum volume of 50 ml and a corresponding lid. 3.3 A desiccator. 3.4 An analytical balance or equivalent, capable of weighing to the nearest 0,1 mg. 4 Test piece 4.1 Each test piece shall comprise an approximately 25 g portion of a sample representative of the material before moulding or extrusion, as applicable, or cut in accordance with the referring standard from a cross section of a pipe or fitting. NOTE. If test samples utilize different sampling weights or are taken from different sources, e.g. raw material granulate or finished product, then there may be a difference in test results obtained. This may depend on e.g. the surface area/mass ratio or the maximum thickness of material. To demonstrate correlation with results for granulate samples determined in accordance with this standard, the preparation of samples from finished product may have to be modified. 4.2 The number of test pieces shall be as specified in the referring standard. 5 Procedure 5.1 Clean and dry a weighing cup and its lid 3.2 until constant weight is achieved and store them in the desiccator 3.3 for at least 0,5 h at room temperature. 5.2 Take the weighing cup and its lid out of the desiccator and determine their combined mass, m0, to the nearest 0,1 mg. Replace the lid in the desiccator. 5.3 Fill the cup with about 25 g portion of the sample and determine the mass, m1of the cup, lid and the test portion to the nearest 0,1 mg. 5.4 Put the weighing cup in the drying oven zone which is kept at 1052 C see 3.1. 5.5 After a period of 655 min, take the weighing cup out of the drying oven and put the cup in the desiccator for at least 1 h at room temperature. 5.6 Cover the cup with the lid. Weigh the cup, lid and residual material to the nearest 0,1 mg, as mass m2. 6 Calculation Calculate the volatile material content, mv, of the test portion using the following equation mv3 106 m12 m2 m12 m0 where mvis the volatile material content in milligrams per kilogram mg/kg at 1052 C; m0is the mass in grams of the empty weighing cup and its lid; m1is the mass in grams of the weighing cup and its lid plus the test portion; m2is the mass in grams of the weighing cup and its lid plus the residual material after 1 h at 1052 C. 7 Test report The test report shall include the following ination a the reference to this standard and to the referring standard; b the complete identification of the test piece; c the source and of the material; d the test temperature; e the number of test portions tested; f the calculated volatile material content, in milligrams per kilogram mg/kg for each test portion; g any factors which may have affected the results, such as any incidents or any operating details not specified in this standard; h the date of the test. w w w . b z f x w . c o m BSI 389 Chiswick High Road London W4 4AL | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | BSI British Standards Institution BSI is the independent national body responsible for preparing British Standards. 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