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BS EN ISO 136782009 ICS 75.180.10, NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW BRITISH STANDARD Petroleum and natural gas industries uation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements ISO 136782009 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 June 2009 BSI 2009 ISBN 978 0 580 56640 0 Amendments/corrigenda issued since publication Date Comments BS EN ISO 136782009 National foreword This British Standard is the UK implementation of EN ISO 136782009. It is identical to ISO 136782009. It supersedes BS ISO 136782000 which is withdrawn. The UK participation in its preparation was entrusted to Technical Committee PSE/17/-/5, Casing, tubing and drill pipe. A list of organizations represented on this committee can be obtained on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13678 May 2009 ICS 75.180.10 English Version Petroleum and natural gas industries - uation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements ISO 136782009 Industries du ptrole et du gaz naturel - valuation et essais des graisses pour filetage utilises pour les tubes de cuvelage, les tubes de production, les tubes de conduites et les lments de garnitures de forage ISO 136782009 Erdl- und Erdgasindustrie - Beurteilung und Prfung von Gewindefetten zur Verwendung an Futter-, Steig- und Leitungsrohren und an Bohrgestngeteilen ISO 136782009 This European Standard was approved by CEN on 30 April 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official versions English, French, German. A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre Avenue Marnix 17, B-1000 Brussels 2009 CENAll rights of exploitation in any and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 136782009 E BS EN ISO 136782009 EN ISO 136782009 E Foreword This document EN ISO 136782009 has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by November 2009, and conflicting national standards shall be withdrawn at the latest by November 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 136782009 has been approved by CEN as a EN ISO 136782009 without any modification. BS EN ISO 136782009 ISO 136782009E ISO 2009 – All rights reserved iii Contents Page Foreword............................................................................................................................................................ iv Introduction........................................................................................................................................................ v 1 Scope ......................................................................................................................................................1 2 Conance..........................................................................................................................................1 2.1 Dual citing of normative references.....................................................................................................1 2.2 Units of measurement...........................................................................................................................1 3 Normative references............................................................................................................................2 4 Terms and definitions ...........................................................................................................................3 5 Thread compound characteristics.......................................................................................................4 5.1 Product characteristics.........................................................................................................................4 5.2 Physical and chemical characteristics................................................................................................5 6 Thread compound perance properties........................................................................................9 6.1 Small-scale test......................................................................................................................................9 6.2 Frictional properties..............................................................................................................................9 6.3 Extreme surface-contact pressure gall resistance properties for casing, tubing and line pipe........................................................................................................................................................10 6.4 Fluid sealing properties for casing, tubing and line pipe................................................................11 7 Quality assurance and control...........................................................................................................11 8 Marking requirements .........................................................................................................................12 8.1 Marking.................................................................................................................................................12 8.2 Labelling ...............................................................................................................................................12 Annex A inative API modified thread compound.................................................................................13 Annex B normative Casing, tubing and line pipe reference standard ulation .................................17 Annex C normative Penetration test.............................................................................................................19 Annex D normative Evaporation test............................................................................................................20 Annex E normative Oil separation test.........................................................................................................21 Annex F normative Application/adherence test ..........................................................................................22 Annex G normative Gas evolution test.........................................................................................................23 Annex H normative Water leaching test.......................................................................................................27 Annex I inative Frictional properties test .............................................................................................30 Annex J inative Extreme surface-contact pressure galling test for casing, tubing and line pipe........................................................................................................................................................40 Annex K inative Fluid sealing test for casing, tubing and line pipe..................................................41 Annex L inative Corrosion inhibition tests...........................................................................................44 Annex M inative Compound high-temperature stability test..............................................................45 Bibliography......................................................................................................................................................46 BS EN ISO 136782009 ISO 136782009E iv ISO 2009 – All rights reserved Foreword ISO the International Organization for Standardization is a worldwide federation of national standards bodies ISO member bodies. The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission IEC on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13678 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 5, Casing, tubing and drill pipe. This second edition cancels and replaces the first edition ISO 136782000, which has been technically revised. It is the intent of ISO/TC 67 that the first and second editions of ISO 13678 both be applicable, at the option of the purchaser, for a period of six months from the first day of the calendar quarter immediately following the date of publication of this second edition, after which period the first edition will no longer be applicable. BS EN ISO 136782009 ISO 136782009E ISO 2009 – All rights reserved v Introduction This International Standard is based on API RP 5A3 [5], second edition, July 2003, with errata and inclusion of all clauses of API RP 7A11 [6], first edition, November 1992, incorporated into Annex I. This International Standard specifies requirements and gives recommendations for the manufacture, testing and selection of thread compounds for use on casing, tubing, line pipe and drill stem elements based on the current industry consensus of good engineering practice. It is intended that the words casing and tubing apply to the service application, rather than to the diameter of the pipe. The perance requirements of thread compounds for use with casing, tubing, line pipe, premium connections and rotary shouldered connections include ⎯ consistent frictional properties that allow both proper and uni connection engagement; ⎯ adequate lubrication properties to resist galling or damage of connection contact surfaces during make-up and breakout; ⎯ adequate sealing properties for thread-type seal connections and/or not inhibiting the sealing properties of non-thread sealing connections e.g. metal-to-metal seals, polytetrafluoroethylene PTFE seals, etc. depending upon service requirements; ⎯ physical and chemical stability both in service and in expected compound storage conditions; ⎯ properties that allow effective application to the connection contact surfaces in expected service conditions and environment. In addition, compounds for rotary shouldered connections provide ⎯ lubrication of the connection members during make-up to achieve the proper axial bearing stress; ⎯ an effective seal between connection shoulders to prevent wash-out by drilling fluids; ⎯ more uni distribution of circumferential bearing stress if shoulders are not parallel; ⎯ resistance to additional make-up down hole. When uating the suitability of a thread compound, the user can define the service conditions and then consider field trials and field service experience in addition to laboratory test results. Appropriate supplementary tests can be utilized for specific applications which are not uated by the tests herein. The user and manufacturer are encouraged to discuss service applications and limitations of the compound being considered. Representatives of users and/or other third party personnel are encouraged to monitor tests wherever possible. Interpolation and extrapolation of test results to other products, even of similar chemical composition, is not recommended. 1 Obsolete. Incorporated into this International Standard. BS EN ISO 136782009 ISO 136782009E vi ISO 2009 – All rights reserved Testing in compliance with this International Standard does not in and of itself ensure adequate thread compound/connection system perance in field service. The user has the responsibility of uating the results obtained from the recommended procedures and test protocols and determining
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